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HPLC determination of glyoxal in aldehyde solution with 3-methyl-2-benzothiazolinone hydrazone
Yamei ZHU, Xiaoli YAO, Shaohui CHEN, Qun CUI, Haiyan WANG
《化学科学与工程前沿(英文)》 2011年 第5卷 第1期 页码 117-121 doi: 10.1007/s11705-010-0535-4
关键词: HPLC glyoxal 3-methyl-2-benzothiazolinone hydrazone diazine dicarbonyl compounds
Encapsulation of 2-amino-2-methyl-1-propanol with tetraethyl orthosilicate for CO2 capture
Sidra Rama, Yan Zhang, Fideline Tchuenbou-Magaia, Yulong Ding, Yongliang Li
《化学科学与工程前沿(英文)》 2019年 第13卷 第4期 页码 672-683 doi: 10.1007/s11705-019-1856-6
关键词: carbon capture microencapsulated sorbents emulsion technique low temperature adsorption and absorption
Photocatalytic degradation of methyl orange using ZnO/TiO composites
Ming GE , Changsheng GUO , Xingwang ZHU , Lili MA , Wei HU , Yuqiu WANG , Zhenan HAN ,
《环境科学与工程前沿(英文)》 2009年 第3卷 第3期 页码 271-280 doi: 10.1007/s11783-009-0035-2
关键词: photocatalytic degradation methyl orange ZnO/TiO2 composites high performance liquid chromatography mass spectrometry (HPLC-MS)
XIAO Xinyan, ZHANG Huiping, CHEN Huanqin, LIAO Dongliang
《化学科学与工程前沿(英文)》 2007年 第1卷 第2期 页码 178-183 doi: 10.1007/s11705-007-0033-5
关键词: prepared photocatalytic activity apparent photocatalytic orthogonal
Methyl acetate–methanol mixture separation by extractive distillation: Economic aspects
Elena Graczová, Branislav Šulgan, Samuel Barabas, Pavol Steltenpohl
《化学科学与工程前沿(英文)》 2018年 第12卷 第4期 页码 670-682 doi: 10.1007/s11705-018-1769-9
Methyl acetate is considered low toxicity volatile solvent produced either as a by-product during methanol carbonylation or via acetic acid esterification with methanol. In both cases, pure methyl acetate has to be isolated from the reaction mixture. Simulation of methyl acetate separation from its mixture with methanol by extraction distillation was carried out in ASPEN+ software. In total three case studies were assumed using two different extraction solvents and two solvent regeneration strategies. In case A, novel extraction solvent 1-ethyl-3-methylimidazolium trifluoromethanesulfonate ionic liquid, was considered. Raw material separation was achieved in an extraction distillation column while the solvent regeneration was accomplished in a second distillation column in this case. In case study B, the same extraction solvent was used; however, its regeneration was carried out in a single-effect evaporator. Dimethyl sulfoxide was the second extraction solvent selected. Its use in methyl acetate-methanol separation is presented in case study C. As high purity of dimethyl sulfoxide was required for the methyl acetate-methanol azeotrope breaking, its regeneration was carried out in the second distillation column only. To simulate the ternary methyl acetate–methanol–extraction solvent mixtures separation, vapor–liquid equilibrium was predicted based on the NRTL equation. Further, unknown properties of the considered ionic liquid and variation of these properties with temperature were predicted and introduced into the ASPEN+ components properties database. Based on these data, optimum operation parameters of the respective separation equipment were established. In all case studies, the same condition had to be fulfilled, namely minimum methyl acetate content in the distillate from the extraction distillation column of 99.5mol-%. Results of simulations using the respective optimum operation parameters were employed in the economic evaluation of the three separation unit designs studied. It was found that the least energy-demanding design corresponds to the case study B in terms of both capital as well as operation expenses.
关键词: methyl acetate 1-ethyl-3-methylimidazolium trifluoromethanesulfonate extraction distillation dimethyl sulfoxide economic evaluation
YE Lin, ZHAO Yumei, FENG Zengguo, BAI Ying, WU Feng
《化学科学与工程前沿(英文)》 2007年 第1卷 第4期 页码 343-348 doi: 10.1007/s11705-007-0062-0
关键词: 4-butanediol 2-methoxyethylenoxy consistent oxetane-derived copolymer
《化学科学与工程前沿(英文)》 2023年 第17卷 第12期 页码 2061-2073 doi: 10.1007/s11705-023-2366-0
关键词: organogelator tetraphenylvinyldrazone single crystal aggregation-induced emission effect ion sensing
Biodegradation of 2-methylisoborneol by bacteria enriched from biological activated carbon
Rongfang YUAN, Beihai ZHOU, Chunhong SHI, Liying YU, Chunlei ZHANG, Junnong GU
《环境科学与工程前沿(英文)》 2012年 第6卷 第5期 页码 701-710 doi: 10.1007/s11783-011-0367-6
关键词: 2-methylisoborneol (2-MIB) biodegradation 2-methylenebornane 2-methyl-2-bornane pseudo-first-order reaction
Mayenite supported perovskite monoliths for catalytic combustion of methyl methacrylate
Zekai ZHANG, Zhijian KONG, Huayan LIU, Yinfei CHEN
《化学科学与工程前沿(英文)》 2014年 第8卷 第1期 页码 87-94 doi: 10.1007/s11705-014-1410-5
关键词: mayenite perovskite catalytic combustion methyl methacrylate monolith
Jihong LU, Danfeng ZHANG, Qian CHEN, Buwei YU
《化学科学与工程前沿(英文)》 2011年 第5卷 第1期 页码 19-25 doi: 10.1007/s11705-010-0546-1
关键词: late transition metal catalyst methyl methacrylate polymerization salicylaldiminato nickel complexes methylaluminoxane syndiotactic structure
The stabilization effect of Al2O3 on unconventional Pb/SiO2 catalyst
《化学科学与工程前沿(英文)》 2023年 第17卷 第10期 页码 1423-1429 doi: 10.1007/s11705-023-2315-y
关键词: Pb/SiO2 Al2O3 propane dehydrogenation propene stability
《化学科学与工程前沿(英文)》 2022年 第16卷 第3期 页码 443-460 doi: 10.1007/s11705-021-2079-1
关键词: Stöber method carbon-coated Ni-Co alloy in-situ hydrodeoxygenation methyl palmitate decarbonylation/decarboxylation
Rh2O3/hexagonal CePO4 nanocatalysts for N2O decomposition
Huan Liu, Zhen Ma
《化学科学与工程前沿(英文)》 2017年 第11卷 第4期 页码 586-593 doi: 10.1007/s11705-017-1659-6
关键词: Rh2O3 CePO4 N2O decomposition
GAO Shihao, SUN Chenghui, ZHAO Xinqi, GAO Changquan
《化学科学与工程前沿(英文)》 2008年 第2卷 第1期 页码 80-84 doi: 10.1007/s11705-008-0017-0
关键词: 5-Amino-1 2 4-thiadiazol-3-yl 1 2-dichloroethane important intermediate 2-benzothiazolyl thioester temperature
Xiaohong LI, Wenying LI,
《化学科学与工程前沿(英文)》 2010年 第4卷 第2期 页码 142-146 doi: 10.1007/s11705-009-0233-2
关键词: desorption different TiO-AlOmixed physisorption ethylbenzene
标题 作者 时间 类型 操作
HPLC determination of glyoxal in aldehyde solution with 3-methyl-2-benzothiazolinone hydrazone
Yamei ZHU, Xiaoli YAO, Shaohui CHEN, Qun CUI, Haiyan WANG
期刊论文
Encapsulation of 2-amino-2-methyl-1-propanol with tetraethyl orthosilicate for CO2 capture
Sidra Rama, Yan Zhang, Fideline Tchuenbou-Magaia, Yulong Ding, Yongliang Li
期刊论文
Photocatalytic degradation of methyl orange using ZnO/TiO composites
Ming GE , Changsheng GUO , Xingwang ZHU , Lili MA , Wei HU , Yuqiu WANG , Zhenan HAN ,
期刊论文
Synthesis of TiO2 nano-particles and their photocatalytic activity for formaldehyde and methyl orange
XIAO Xinyan, ZHANG Huiping, CHEN Huanqin, LIAO Dongliang
期刊论文
Methyl acetate–methanol mixture separation by extractive distillation: Economic aspects
Elena Graczová, Branislav Šulgan, Samuel Barabas, Pavol Steltenpohl
期刊论文
Synthesis of copolymers of 3-acryloyloxymethyl-3′-methyloxetane and 3-(2-(2-(2-Methoxyethylenoxy)ethylenoxy)ethylenoxy)-3′-methyloxetane and their ionic conductivity properties
YE Lin, ZHAO Yumei, FENG Zengguo, BAI Ying, WU Feng
期刊论文
Synthesis and ultraviolet/aggregation-induced emission investigation of novel tetraphenylvinyl hydrazone
期刊论文
Biodegradation of 2-methylisoborneol by bacteria enriched from biological activated carbon
Rongfang YUAN, Beihai ZHOU, Chunhong SHI, Liying YU, Chunlei ZHANG, Junnong GU
期刊论文
Mayenite supported perovskite monoliths for catalytic combustion of methyl methacrylate
Zekai ZHANG, Zhijian KONG, Huayan LIU, Yinfei CHEN
期刊论文
Polymerization of methyl methacrylate catalyzed by mono-/bis-salicylaldiminato nickel(II) complexes and
Jihong LU, Danfeng ZHANG, Qian CHEN, Buwei YU
期刊论文
Carbon-coated Ni-Co alloy catalysts: preparation and performance for aqueous phase hydrodeoxygenation of methyl
期刊论文
Improvement in the synthesis of 2-(5-amino-1,2,4-thiadiazol-3-yl)-2-(Z)-methoxyiminoacetic acid 2-benzothiazolyl
GAO Shihao, SUN Chenghui, ZHAO Xinqi, GAO Changquan
期刊论文